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Prepare a buffer by direct addition Consider how best to prepare one liter of a

ID: 705574 • Letter: P

Question

Prepare a buffer by direct addition Consider how best to prepare one liter of a buffer solution with pH- 4.68 using one of the weak acid/conjugate base systems shown here Weak Acid ??,04 H2PO4 HCO3 Conjugate Base C20,2 ? ??,2 ??? Ka 6.4 x 10-5 6.2 x 10-8 4.8 x 10-11 pKa 4.19 7.21 10.32 How many grams of the potassium salt of the weak acid must be combined with how many grams of the potassium salt of its conjugate base, to produce 1.00 L of a buffer that is 1.00 M in the weak base? grams potassium salt of weak acid- grams potassium salt of conjugate base-

Explanation / Answer

Answer

Suitable weak acid and conjucate base combination is HC2O4-/C2O42-

mass of KHC2O4 required = 41.460g

mass of K2C2O4 required = 166.21g

Explanation

HC2O4-/C2O42- is the suitable buffer for the target pH 4.68

because pKa is near to the target pH

Henderson-Hasselbalch equation is

pH = pKa + log([A-] /[HA])

where,

[A-] =[ C2O42-] = 1.00M

[HA]= [HC2O4-]

pKa = 4.19

4.68 = 4.19 + log([C2O42-] /[HC2O4-])

log([C2O42-] /[HC2O4-]) = 0.49

[C2O42-] /[HC2O4-] = 3.09

given concentration of C2O42- = 1.00M

   HC2O4- = 1.00/3.09 = 0.3236

Volume of buffer = 1.00L

Therefore

  moles of KHC2O4 required = 0.3236

moles of K2C2O4 required = 1.00

   molar mass of KHC2O4 = 128.12g/mol

mass of KHC2O4 required = 128.12g/mol × 0.3236mol = 41.460g

molar mass of K2C2O4 = 166.21g/mol

mass of K2C2O4 required = 166.21g/mol × 1.00mol = 166.21g