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In a similar experiment to the one being performed in the lab, 1.44 g of ammoniu

ID: 795286 • Letter: I

Question

In a similar experiment to the one being performed in the lab, 1.44 g of ammonium chloride (MM = 53.49 g/mol, D = 1.53 g/mL) is reacted with 3.81 mL of t-butanol (MM = 74.12 g/mol, D = 0.78 g/mL) to form t-butyl chloride (MM = 92.57 g/mol).  After the reaction 2.15 g of t-butyl chloride is synthesized.  Find the limiting reagent, theoretical yield and percent yield of t-butyl chloride.  Note that in the actual experiment you will have two nucleophiles making it impossible to find theoretical yield.

Limiting Reagent = <--Make sure you have the correct spelling (including spaces and dashes as necessary).  All compound names are spelled out in the question above.
Theoretical Yield = g
Percentage Yield = %

Explanation / Answer


ammonium chloride + t-butanol => t-butyl chloride + ammonium hydroxide

Theoretical moles of ammonium chloride : t-butanol = 1 : 1


Moles of ammonium chloride = mass/molar mass = 1.44/53.49 = 0.026921 mol

Moles of t-butanol = volume x density/molar mass = 3.81 x 0.78/74.12 = 0.040094 mol

Experimental moles of ammonium chloride : t-butanol = 0.026921 : 0.040094 = 1 : 1.4893


Since t-butanol is in excess => ammonium chloride is the limiting reagent


Moles of t-butyl chloride = moles of ammonium chloride = 0.026921 mol

Theoretical yield = moles x molar mass of t-butyl chloride

= 0.026921 x 92.57

= 2.492 g = 2.49 g


Percentage Yield = actual yield/theoretical yield x 100%

= 2.15/2.492 x 100%

= 86.3%


Thus:

Limiting Reagent = ammonium chloride

Theoretical Yield = 2.49 g

Percentage Yield = 86.3%