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Here\'s the part 1 info Using the calculations from your prelab, prepare 100 mL

ID: 884282 • Letter: H

Question

Here's the part 1 info

Using the calculations from your prelab, prepare 100 mL of 0.25M Tris and 100 mL 0.25M Tris-HCl. Be sure to use the 10 mM KCl provided as the solvent.

Using the solutions you just made, create 10 mL samples of the following buffer ratios:

100% Tris-HCl

75% Tris-HCl, 25% Tris

50% Tris-HCl, 50% Tris

25% Tris-HCl, 75% Tris

100% Tris

Complete the following table using the molarities you calculated for each buffer in Part 1. Using a 10 mL aliquot of the buffer, show the change in mmoles when 0.01 mL of 2.0M HCl is added to the buffer. Predict the change in pH after the addition.


Complete the following table using the molarities you calculated for each buffer in Part 1. Using a 10 mL aliquot of the buffer, show the change in mmoles when 0.01 mL of 2.0M NaOH is added to the buffer. Predict the change in pH after the addition.

Buffer # Initial moles of Tris-HCL Initial moles of Tris Post Addition of HCL
mmol of Tris-HCl Post Addition of HCL
mmol of Tris Predicted pH Buffer 1 0.0001875 6.25e-05
1
2
3 Buffer 2 0.000125 0.000125
4
5
6 Buffer 3 8.75e-05 0.0001625
7
8
9

Explanation / Answer

0.01 mL of 2.0M HCl =0.00002 moles=0.02mmol

the blanks=

1) 0.1875mmoles+0.02mmol=0.2075 mmol

2)6.25e-05-0.00002 moles=4.25e^-05moles=0.0425mmol

3) pH=Pka + log [base]/[acid]=8.214 + log 0.0425/0.2075=7.5254

4) 0.125+0.02mmol=0.145mmol

5)0.125-0.02mmol=0.105mmol

6)pH=8.314+log [0.105]/0.145=8.214-0.1402=8.0738

7)8.75e-02mmol+0.02mmol=0.1075mmol

8)0.1625mmol-0.02mmol=0.1425mmol

9)pH=8.214+ log 0.1425/0.1075=8.3363

table 2

0.01 mL of 2.0M NaOH=0.00002 moles=0.02mmol

10)0.1875mmoles-0.02mmol=0.1675mmol

11)6.25e-05+0.00002 moles=4.25e^-05moles=0.0825mmol

12) pH=8.314+log0.0825/0.1675=7.9064

13)0.125-0.02mmol=0.105mmol

14)0.125-0.02mmol=0.145mmol

15)pH=8.314+log [0.145]/0.105=8.214-0.1402=8.3309

16)8.75e-02mmol-0.02mmol=0.0675mmol

17)0.1625mmol+0.02mmol=0.1825mmol

18)pH=8.214+ log 0.1825/0.0675=8.6457