Academic Integrity: tutoring, explanations, and feedback — we don’t complete graded work or submit on a student’s behalf.

Show all work and answer the following using the correct number of significant f

ID: 229688 • Letter: S

Question

Show all work and answer the following using the correct number of significant figures. [Note: Since this is a take-home quiz and aren't limited by class time, if you need to use the quadratic equation, I expect you do actually do the calculation.] (10 pts) Carbonic acid (H2CO3, Kal = 4.46 x 10-7,Ka2-4.69 x 10-11) is a diprotic acid. A titration is performed when 25.00 mL of 0.1250 M disodium carbonate (Na2C03) is reacted with 0.1535 M HCI. What is the pH at the following points along the titration curve? [Attach a separate sheet if necessary.] a) The initial pH b) 5.00 mL before the first equivalence point c) At the first equivalence point d) 5.00 mL after the first equivalence point e) At the second equivalence point f 1.00 mL after the second equivalence point

Explanation / Answer

CO3^2- + H+ <==> HCO3- ..... Kb1 = Kw/Ka2 = 1 x 10^-14/4.69 x 10^-11 = 2.13 x 10^-4

HCO3- + H+ <==> H2CO3 ..... Kb2 = Kw/Ka1 = 1 x 10^-14/4.46 x 10^-7 = 2.24 x 10^-8

pKa1 = -log(4.46 x 10^-7) = 6.35

pKa2 = -log(4.69 x 10^-11) = 10.33

a) initial

[CO3^2-] = 0.125 M

hydrolysis reaction,

CO3^2- + H2O <==> HCO3- + OH-

let x amount has hydrolyzed

Kb1 = [HCO3-][OH-]/[CO3^2-]

2.13 x 10^-4 = x^2/0.125

x = [OH-] = 5.16 x 10^-3 M

pOH = -log(5.16 x 10^-3) = 2.29

pH = 14 - 2.29 = 11.71

b) 5 ml before Ist equivalence point

Volume HCl needed to reach Ist equivalence point = 0.125 M x 25 ml/0.1535 M = 20.36 ml

So,

volume HCl added = 15.36 ml

initial moles CO3^2- = 0.125 M x 25 ml = 3.125 mmol

HCl added = 0.1535 M x 15.36 ml = 2.358 mmol

(HCO3-) formed = 2.358 mmol

(CO3^2-) remained = 0.767 mmol

Using Hendersen-Hasselbalck equation,

pH = pKa2 + log(CO3^2-/HCO3-)

     = 10.33 + log(0.767/2.358)

     = 9.84

c) at Ist equivalence point

all of CO3^2- has reacted to form HCO3-

pH = 1/2(pKa1 + pKa2)

      = 1/2(6.35 + 10.33)

      = 8.34

d) 5 ml after Ist equivalence point

Volume HCl needed to reach Ist equivalence point = 0.125 M x 25 ml/0.1535 M = 20.36 ml

So,

volume HCl added = 25.36 ml

initial moles CO3^2- = 0.125 M x 25 ml = 3.125 mmol

HCl added = 0.1535 M x 25.36 ml = 3.893 mmol

(H2CO3) formed = 0.767 mmol

(HCO3-) remained = 2.358 mmol

Using Hendersen-Hasselbalck equation,

pH = pKa2 + log(CO3^2-/HCO3-)

     = 6.35 + log(2.358/0.767)

     = 6.84

e) at IInd equivalence point

all of HCO3- has reacted to form H2CO3

[H2CO3] formed = 0.125 M x 25 ml/(2 x 20.36 ml) = 0.077 M

Dissociation of weak acid

H2CO3 + H2O <==> H3O+ + HCO3-

let x amount dissociated

Ka1 = [HCO3-][H3O+]/[H2CO3]

4.46 x 10^-7 = x^2/0.077

x = [H3O+] = 1.85 x 10^-4 M

pH = -log[H3O+] = 3.73

f) 1.00 ml after IInd equivalence point

excess [H+] = 0.1535 M x 1.0 ml/41.72 ml = 0.0037 M

pH = -log[H+] = -log(0.0037) = 2.43