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Piperazine, C4H10N2, is a diprotic weak base (pKb1 = 4.22 and pKb2 = 8.67). A sa

ID: 818123 • Letter: P

Question

Piperazine, C4H10N2, is a diprotic weak base (pKb1 = 4.22 and pKb2 = 8.67). A sample of piperazine is dissolved in 100.0 mL of water and titrated with 0.500 M HCl. It takes 48.00 mL of HCl to reach the second equivalence point.


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a) What was the original concentration of the piperazine solution?

b) Calculate the pH after the following amounts of HCl have been added: 0 mL, 12.00mL, 24.00mL,36.00mL, 48.00mL, and 60.00mL

c) Sketch the titration curve for this titration

d) Which of the ollowing indicators could be used to detect the first equivalence point? The second?

     Indicator                              Ka                         Color Change

     ______________________________________________________________

     Bromocresol green             2.5 x 10^-5             yellow => blue-green

     Phenol Red                         2.5 x 10^-8            yellow => red

     Methyl Yellow                     3.5 x 10^-4             red     => yellow

     Alizarin Yellow                     8.9 x 10^-12          yellow => red

Explanation / Answer

Chemical reaction: C4H10N2 (aq) + H+ (aq) ----------------> C4H10N2H+(aq) ( First equivalence point) C4H10N2H+(aq) + H+ (aq) ----------------> C4H10N2H2+(aq) (Second equivalence point) From the balanced chemical reacion one mole of the acid isreacting with one mole of the base. We know that the volume required to reach the first equivalence point and thesecond equivalence point is same. Hence the volume of HCl at the first equivalencepoint = 24.0 mL Data: [HCl] = 0.500 M VHCl = 24.0 mL =0.024 L Number of moles of HCl = 0.024 L * 0.500 M =0.012 moles ? Concentration of Piperazine in 100 mL = 0.012 moles /0.1 L = 0.12 M

Chemical reaction: C4H10N2 (aq) + H+ (aq) ----------------> C4H10N2H+(aq) ( First equivalence point) C4H10N2H+(aq) + H+ (aq) ----------------> C4H10N2H2+(aq) (Second equivalence point) From the balanced chemical reacion one mole of the acid isreacting with one mole of the base. We know that the volume required to reach the first equivalence point and thesecond equivalence point is same. Hence the volume of HCl at the first equivalencepoint = 24.0 mL Data: [HCl] = 0.500 M VHCl = 24.0 mL =0.024 L Number of moles of HCl = 0.024 L * 0.500 M =0.012 moles ? Concentration of Piperazine in 100 mL = 0.012 moles /0.1 L = 0.12 M