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Mass of salicylic acid used: 2.0 g Volume of acetic anhydride used: 5:0 g Mass o

ID: 992631 • Letter: M

Question

Mass of salicylic acid used: 2.0 g Volume of acetic anhydride used: 5:0 g Mass of aspirin obtained: 1.47 g Mass of acetic anhydride used: 5.4 g density=1.08 g/mL Melting point of aspirin: 140C How would I find the theoretical yield of aspirin and the percentage yield of aspirin(by mass)? Mass of salicylic acid used: 2.0 g Volume of acetic anhydride used: 5:0 g Mass of aspirin obtained: 1.47 g Mass of acetic anhydride used: 5.4 g density=1.08 g/mL Melting point of aspirin: 140C How would I find the theoretical yield of aspirin and the percentage yield of aspirin(by mass)? Volume of acetic anhydride used: 5:0 g Mass of aspirin obtained: 1.47 g Mass of acetic anhydride used: 5.4 g density=1.08 g/mL Melting point of aspirin: 140C How would I find the theoretical yield of aspirin and the percentage yield of aspirin(by mass)?

Explanation / Answer

acetic anhydride+ salicylic acid ------->acetylsalicylic acid + acetic acid

C4H6O3 + C7H6O3 ------> C9H8O4 + C2H4O2

Molar mass of acetic anhydride is 102 g/mol

Molar mass of salicylic acid is 138 g/mol

Molar mass of acetylsalicylic acid is 180 g/mol

According to the balanced reaction,

102 g of acetic anhydride reacts with 138 g of salicylic acid

M g of acetic anhydride reacts with 2.0 g of salicylic acid

M = ( 2.0x102) / 138

   = 1.48 g

So 5.0-1.48 = 3.52 g of acetic anhydride left unreacted so it is the excess reactant.

Since all the mass of salicylic acid completly reacted it is the limiting reacted.

From the balanced reaction,

138 g of salicylic acid produces 180 g of aspirin

2.0 g of salicylic acid produces Ng of aspirin

N = ( 2.0x180) / 138

   = 2.61 g of asprin ----> this is the theoretical yield

Given actual yield is 1.47 g

So percentage of aspirin = ( acutal yield / theoretical yield) x100

                                    = ( 1.47 / 2.61) x100

                                   = 56.35%